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http://142.54.178.187:9060/xmlui/handle/123456789/19971| Title: | Microwave Assistant Synthesis, Crystal Structure and Biological Activity of A 1,2,4-Triazole Compound |
| Authors: | WEI KE NA-BO SUN HONG-KE WU |
| Keywords: | 1,2,4-triazole synthesis herbicidal activity |
| Issue Date: | 9-Aug-2013 |
| Publisher: | HEJ Research Institute of Chemistry, University of Karachi, Karachi. |
| Citation: | Ke, W., & Sun, N. B. (2013). Microwave assistant synthesis, crystal structure and biological activity of a 1, 2, 4-triazole compound. Journal of the Chemical Society of Pakistan, 35(4), 1241-1246. |
| Abstract: | The title compound (C₁₇H₁₄F₂N₄SO) were synthesized and recrystallized from CH₃CN. The compound was characterized by ¹H-NMR, FTIR, MS, HRMS and X-ray diffraction. The compound crystallized in the Monoclinic space group C2/c with a = 27.532(6), b = 8.9596(18), c = 14.609(3) Å, α = 90, β = 112.59(3), γ =90°, V = 3327.1(12) Å3, Z = 8 and R = 0.0327 for 2596 observed reflections with I > 2σ(I). X-ray analysis reveals that not only intermolecular N–H•••N interactions, but also C-H•••π stacking interactions exist in the adjacent molecules. The biological activities results showed that it exhibited significant herbicidal activity towards Brassica napus. |
| URI: | http://142.54.178.187:9060/xmlui/handle/123456789/19971 |
| ISSN: | 0253-5106 |
| Appears in Collections: | Issue 04 |
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